Macylab：The experimental scheme of icp6800 for the determination of Si, Mn, P, Cr, Mo, Ni and Cu in
Macylab：The experimental scheme of icp6800 for the determination of Si, Mn, P, Cr, Mo, Ni and Cu in steel
1. Preface
With the development and application of metal products, it is closely related to human production and life. Therefore, more and more stringent testing standards and requirements are put forward for products and raw materials. Traditional chemical analysis methods can not meet the requirements of daily analysis and testing. ICP-AES inductively coupled plasma atomic emission spectrometer is widely used in the determination of elements in metal industry because of its low detection limit, fast testing speed, high resolution and high accuracy.
P1. ICP6800.Inductively coupled plasma atomic emission spectrometer
P2.Application examples
2. Product introduction
ICP6800 inductively coupled plasma single channel scanning emission spectrometer has excellent resolution, accuracy and precision. It is widely used in rare earth industry, petrochemical industry, ore analysis, metal smelting, geological research, drug safety, experimental research, environmental detection, food safety and other industries. Especially for the determination of element content in hardware industry, icp6800 has many successful cases. Table 1 shows the main technical parameters of icp6800.
|
RF generator |
|
|
working frequency |
27.12MHz |
|
Frequency stability |
﹤0.05％ |
|
output power |
800W ～1600W |
|
Output power stability |
≤0.05％ |
|
Matching method |
Automatic matching |
|
Scanning beam splitter |
|
|
light path |
Czerny turner |
|
Focus |
1000mm |
|
Grating specification |
Ion etched holographic grating, etched line density :3600L/mm or 2400L/mm；ruled area（80×110）mm |
|
Reciprocal of linear dispersion |
0.26nm/m |
|
resolving power |
≤0.008nm(3600 Line grating） |
|
≤0.015nm(2400 Line grating) |
|
|
Technical index of the whole machine |
|
|
Scanning wavelength range |
195nm～500nm（3600L/mm grating） |
|
195nm～800nm（2400L/mm grating） |
|
|
Repeatability |
RSD≤1.5％ |
|
stability |
RSD≤2.0％ |
Table 1. Main technical parameters of icp6800
3、 Evaluation of measurable elements in samples
According to the customer's samples and relevant information, through consulting the relevant data and standards, it is evaluated that the customer's samples can be accurately tested by the analyzer. The details are shown in Table 2
|
Sample |
Measuring elements |
Macylab instrument |
Overview of sample handling (for reference only) |
remarks |
|
Metal material |
Si, Mn, P, Cr, Mo, Ni, Cu |
ICP6800
|
Weigh about 0.2-0.5g sample, add a certain amount of nitric acid, heat at low temperature, after the solution is clear, remove and cool to room temperature, transfer it into a 100ml volumetric flask, dilute it to the scale with water, and mix well. |
In order to determine the content of silicon accurately, blank and parallel sample experiments are needed. |
4、 Instrument configuration:
Table 3 shows the instrument configuration required for sample determination, including instrument host, accessories, sample pretreatment equipment, reagents, etc.
|
Instrument host and necessary accessories |
||||||
|
Serial number |
name |
specification / model |
manufacturer |
quantity |
remarks |
|
|
1 |
Inductively coupled plasma atomic emission spectrometer |
ICP6800 |
Shanghai Macylab Instrument Co., Ltd |
1 |
|
|
|
2 |
automatic temperature control circulating cooling water device |
|
|
1 |
|
|
|
3 |
regulated power supply |
|
|
1 |
|
|
|
Instrument accessories |
||||||
|
Serial number |
name |
specification / model |
manufacturer |
quantity |
remarks |
|
|
1 |
computer host |
|
|
1 |
|
|
|
2 |
computer monitors |
|
|
1 |
|
|
|
3 |
printers |
|
|
1 |
|
|
|
Sample processing equipment and consumables |
||||||
|
Serial number |
name |
specification / model |
manufacturer |
quantity |
remarks |
|
|
1 |
electronic temperature control heating plate |
EG-35B |
|
1 |
|
|
|
2 |
One 10000 electronic balance |
BS224S |
|
1 |
|
|
|
3 |
Laboratory grade ultra pure water machine |
EPED-40T |
|
1 |
|
|
|
4 |
Disposable rubber gloves |
M号 |
|
/ |
|
|
|
5 |
Activated carbon mask |
|
|
/ |
|
|
|
6 |
3ml pipette |
3ml |
|
/ |
|
|
|
7 |
100ml glass beaker |
100ml |
|
/ |
|
|
|
8 |
100ml glass volumetric flask |
100ml |
|
/ |
|
|
|
9 |
5ml pipette gun |
0.5ml-5ml |
|
1 |
|
|
|
10 |
1ml pipette gun |
100ul-1000ul |
|
1 |
|
|
|
11 |
100ul pipette gun |
10ul-100ul |
|
1 |
|
|
|
reagent |
||||||
|
Serial number |
name |
specification / model |
manufacturer |
quantity |
remarks |
|
|
1 |
hydrochloric acid |
superior pure |
|
/ |
|
|
|
2 |
Nitric acid |
superior pure |
|
/ |
|
|
|
3 |
Hydrogen peroxide |
superior pure |
|
/ |
|
|
|
4 |
Each element reference material |
1000ug/ml |
|
/ |
|
|
Table 3. Configuration of icp6800 and related instruments
